Water Quality Testing

Woman working in lab coat in NRRI water chemistry lab.

Lab Overview

Central Analytical Water Testing Lab

The NRRI Central Analytical Laboratory (CAL) has been in operation since 1987, providing analytical services and research support to a wide variety of partners and clients, including University of Minnesota scientists; local, state, tribal, and federal governmental agencies; private businesses; and commercial laboratories. The lab is certified as a water quality testing laboratory under the Minnesota Pollution Control Agency’s Laboratory Certification Program.

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    Water Quality Testing Services

    Physical Analyses

    • Color, apparent (spectrophotometric or visual)  
    • Color, true (add filtration)  
    • Specific Conductivity (µS/cm) 
    • Residue - Filterable (TDS)  
    • Residue - Total Suspended (TSS)  
    • Residue - Total  
    • Residue - Volatile (VSS) (includes TSS) 
    • Turbidity 

    Inorganics, non-metallics 

    • pH (standard)  
    • pH (closed head space)  
    • Acidity  
    • Alkalinity (end point)  
    • ANC (Gran plot)  
    • ANC + pH (closed head space)  
    • Chloride (FIA mercuric thiocyanate FIA ) 
    • Sulfate  
    • Hardness as CaCO3 
    • Nitrogen 
    • Nitrogen Ammonia, dissolved (NH4-N)
    • Nitrate + nitrite (Autoanalyzer) (NO3/NO2-N)
    • Total (TN) 
    • TKN (by calculation; TN minus [NO3/NO2-N])
    • Phosphorus 
      • Phosphate-ortho (OP, or SRP)
      • Phosphorus-Total dissolved (DP)
      • Phosphorus -Total (TP)
      • Bioavailable Sediment TP  
    • TN + TP (simultaneous persulfate digestion) 
    • Silica, dissolved 

    Organics 

    • Carbon, total (TC)  
    • Carbon, total organic (TOC)  
    • Carbon, total organic (TOC), sediment (includes digestion)  
    • Carbon, dissolved organic (DOC)  

    Biological 

    • Chlorophyll-a with phaeophytin (Spectrophotometric or Fluorometric)  
    • Chlorophyll-a + b + c (Trichromatic)  
    • Algal composition analysis (rapid algal scan)  
    • Quantitative algal counts to species (with or without biovolume estimates)  
    • Zooplankton counts  
    • Total Coliforms (mpn)
    • E. Coli (mpn)

    Additional Services  

    • Sample filtration  
    • Digestions, non-routine  
    • Bottle preparation (per bottle)  
    • Bottle charges  
    • Sampling design consultation and development
    • Quality Assurance Project Plan (QAPP) consultation

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    Lab Certifications, Capabilities and Equipment

    Lab Expertise

    The NRRI CAL specializes in the analysis of low-level nutrients and water quality measures commonly encountered in the low nutrient lakes and streams located in the Upper Great Lakes region. Lab members are experts in studying the lakes and streams of northern Minnesota, and have been doing so for 3 decades.

    Lab Certifications

    The NRRI CAL is certified for numerous Clean Water Act and Safe Drinking Water Act water quality measures by the Minnesota Pollution Control Agency. Certification follows National Environmental Laboratory Accreditation Program (NELAP) guidelines and requires annual Proficiency Testing through a secondary agency. The lab also participates in voluntary local, state and federal round robin quality assurance programs each year. 

    NRRI CAL excels at laboratory quality control practices and has extensive experience developing Quality Assurance Program Plans (QAPPs) for state and federally funded projects, including MPCA Surface Water Assessment (SWA) and Water Pollution Load Monitoring Network (WPLMN) Programs, USEPA funded Great Lakes Coastal Wetland Monitoring, and the USEPA funded Great Lakes Sediment Surveillance Program.

    Key Equipment and Capabilities

    • Flow Injection Autoanalyzer: Quantitative analysis of nutrients (low levels of all nitrogen and phosphorus fractions), silica, chloride, and sulfate
    • Narrow band UV/VIS spectrophotometer: Quantitative colorimetric analysis for chlorophyll-a and phaeophytin, true or apparent color, low-level nitrogen and phosphorus
    • Fluorometer: Quantitative analysis of algal pigments (chlorophyll-a and phycocyanin) and water movement tracers
    • Total Organic Carbon Analyzer: Quantitative analysis of total and dissolved organic carbon
    • Turbidimeters (bench and field): Quantitative analysis of turbidity
    • pH meter/titration equipment: Quantitative analysis of alkalinity, acid neutralizing capacity, and hardness
    • IDEXX Quanti-Tray System: Quantitative analysis of E. coli and Total Coliform bacteria
    • Hydrolab and YSI multi-parameter water quality sondes, handheld field displays, Campbell Scientific dataloggers
    • Limnological field sampling equipment for water, plankton, and sediment samples